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Issue 100, 2016, Issue in Progress
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A new multicomponent reaction for direct synthesis of primary γ-nitroamides

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Abstract

A new multicomponent reaction for direct synthesis of γ-nitroamides promoted by ammonium carbonate was developed. A series of γ-nitroamides were synthesized in 35–93% yield from Meldrum's acid, aromatic or aliphatic aldehydes, nitromethane and ammonium carbonate. A mechanistic pathway was proposed based on electrospray ionization mass spectrometry (ESI/MS) experiments.

Graphical abstract: A new multicomponent reaction for direct synthesis of primary γ-nitroamides

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Publication details

The article was received on 04 Sep 2016, accepted on 11 Oct 2016 and first published on 11 Oct 2016


Article type: Paper
DOI: 10.1039/C6RA22141F
Citation: RSC Adv., 2016,6, 98427-98433
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    A new multicomponent reaction for direct synthesis of primary γ-nitroamides

    C. R. Montes D'Oca, J. C. da Silva, E. P. Guedes, M. G. Montes D'Oca, L. S. Santos, F. M. Nachtigall and D. Russowsky, RSC Adv., 2016, 6, 98427
    DOI: 10.1039/C6RA22141F

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