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Issue 26, 2015
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Stepwise synthesis and characterization of germa[4], [5], [8], and [10]pericyclynes

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Abstract

The stepwise syntheses of germa[N]pericyclynes, including [5]pericyclynes, and their characterization are described. The yields of germa[4] and [8]pericyclynes were improved significantly compared to those obtained in previous studies. The routes reported herein afforded the novel germa[5] and [10]pericyclynes, which were characterized by X-ray crystallography, UV-Vis spectroscopy, and fluorescence emission spectroscopy. A unique fluorescence emission was observed for the large germa[10]pericyclyne ring.

Graphical abstract: Stepwise synthesis and characterization of germa[4], [5], [8], and [10]pericyclynes

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Publication details

The article was received on 14 Apr 2015, accepted on 08 May 2015 and first published on 19 May 2015


Article type: Paper
DOI: 10.1039/C5DT01411E
Author version available: Download Author version (PDF)
Citation: Dalton Trans., 2015,44, 11811-11818
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    Stepwise synthesis and characterization of germa[4], [5], [8], and [10]pericyclynes

    H. Tanimoto, T. Nagao, T. Fujiwara, Y. Nishiyama, T. Morimoto, T. Suzuka, K. Tsutsumi and K. Kakiuchi, Dalton Trans., 2015, 44, 11811
    DOI: 10.1039/C5DT01411E

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