Rhenium-catalysed C(sp3)–H bond borylation in the absence of any oxidant, hydrogen acceptor, or external ligand, with the generation of H2 as the sole byproduct is described. The transformation, which represents a rare example of rhenium-catalysed C(sp3)–H bond functionalisation, features high atom efficiency and simple reaction conditions.
The article was received on 28 Nov 2014, accepted on 03 Feb 2015 and first published on 05 Feb 2015
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