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Issue 13, 2015
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A self-assembled, π-stacked complex as a finely-tunable magnetic aligner for biomolecular NMR applications

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Abstract

The number of molecules constituting 1D intermolecular aggregates of the π-stacked self-assembled complex was controlled by altering the concentration and temperature. Enhanced magnetic orientation was observed for the aggregates with larger aggregation numbers. It was demonstrated that the designable complex aggregates serve as magnetic aligners to induce magnetic alignment upon an analyte protein coexisting in the solution, resulting in the observation of residual dipolar coupling (RDC) of the analyte.

Graphical abstract: A self-assembled, π-stacked complex as a finely-tunable magnetic aligner for biomolecular NMR applications

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Publication details

The article was received on 24 Nov 2014, accepted on 20 Dec 2014 and first published on 23 Dec 2014


Article type: Communication
DOI: 10.1039/C4CC09354B
Author version available: Download Author version (PDF)
Citation: Chem. Commun., 2015,51, 2540-2543
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    A self-assembled, π-stacked complex as a finely-tunable magnetic aligner for biomolecular NMR applications

    S. Sato, R. Takeuchi, M. Yagi-Utsumi, T. Yamaguchi, Y. Yamaguchi, K. Kato and M. Fujita, Chem. Commun., 2015, 51, 2540
    DOI: 10.1039/C4CC09354B

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