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Issue 11, 2015
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Dynamic nuclear polarization of a glassy matrix prepared by solid state mechanochemical amorphization of crystalline substances

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Abstract

A mechanochemical “solvent-free” route is presented for the preparation of solid samples ready to be employed in the Dynamic Nuclear Polarization (DNP). 1H-DNP build-up curves at 3.46 T as a function of temperature and radical concentration show steady state nuclear polarization of 10% (0.5% TEMPO concentration at 1.75 K).

Graphical abstract: Dynamic nuclear polarization of a glassy matrix prepared by solid state mechanochemical amorphization of crystalline substances

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Publication details

The article was received on 22 Oct 2014, accepted on 15 Dec 2014 and first published on 17 Dec 2014


Article type: Communication
DOI: 10.1039/C4CC08348B
Author version available: Download Author version (PDF)
Citation: Chem. Commun., 2015,51, 2080-2083
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    Dynamic nuclear polarization of a glassy matrix prepared by solid state mechanochemical amorphization of crystalline substances

    E. Elisei, M. Filibian, P. Carretta, S. Colombo Serra, F. Tedoldi, J. F. Willart, M. Descamps and A. Cesàro, Chem. Commun., 2015, 51, 2080
    DOI: 10.1039/C4CC08348B

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