Oxacalix[4]arene-supported di-, tetra- and undecanuclear copper(II) clusters

Robyn E. Fairbairn; Ross McLellan; Ruaraidh D. McIntosh; Maria A. Palacios; Euan K. Brechin; Scott J. Dalgarno

doi:10.1039/C3DT53088D

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Dalton Transactions

Issue 14, 2014

The international journal for inorganic, organometallic and bioinorganic chemistry

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Oxacalix[4]arene-supported di-, tetra- and undecanuclear copper(II) clusters

Robyn E. Fairbairn,^a Ross McLellan,^a Ruaraidh D. McIntosh,^a Maria A. Palacios,^b Euan K. Brechin*^b and Scott J. Dalgarno*^a

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Institute of Chemical Sciences, Heriot-Watt University, Riccarton, Edinburgh, UK
E-mail: S.J.Dalgarno@hw.ac.uk;
Fax: +44(0)131 451 3180 ;
Tel: +44(0)131 451 8025

EaStCHEM School of Chemistry, University of Edinburgh, West Mains Road, Edinburgh, UK
E-mail: ebrechin@staffmail.ed.ac.uk;
Fax: +44(0)131 650 6453 ;
Tel: +44(0)131 650 7545

Dalton Trans., 2014,43, 5292-5298

DOI: 10.1039/C3DT53088D
Received 31 Oct 2013, Accepted 04 Dec 2013
First published online 12 Dec 2013

This article is part of themed collection: Celebrating the 2014 RSC Prize and Award Winners

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Abstract
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Oxacalix[4]arenes containing either one or two oxa-bridges afford di and undecanuclear Cu^II clusters respectively upon reaction with cupric nitrate under facile conditions. Variation in reaction conditions results in formation of a tetranuclear Cu^II cluster with mono-oxacalix[4]arene, representing a structural expansion of the dinuclear assembly.

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Robyn E. Fairbairn
Ross McLellan
Ruaraidh D. McIntosh
Maria A. Palacios
Euan K. Brechin
Scott J. Dalgarno

Dalton Transactions

Oxacalix[4]arene-supported di-, tetra- and undecanuclear copper(II) clusters

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