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Issue 2, 2014
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Synthesis, structure and spectroscopic analyses of aquachloridooxidodiperoxidomolybdate(VI)

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Abstract

A novel aquachloridooxidodiperoxidomolybdate(VI), [MoClO(O2)2(OH2)], was crystallised as tetraethylammonium and triethylmethylammonium salts from strongly acidic aqueous solutions, and was structurally analysed by single crystal X-ray diffraction and NMR spectroscopy. The aqueous behaviour of the present anion observed by 17O NMR agrees with that reported in a previous speciation study.

Graphical abstract: Synthesis, structure and spectroscopic analyses of aquachloridooxidodiperoxidomolybdate(vi)

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Publication details

The article was received on 10 Oct 2013, accepted on 26 Oct 2013 and first published on 29 Oct 2013


Article type: Communication
DOI: 10.1039/C3DT52848K
Citation: Dalton Trans., 2014,43, 402-405
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    Synthesis, structure and spectroscopic analyses of aquachloridooxidodiperoxidomolybdate(VI)

    M. Saito and M. Hashimoto, Dalton Trans., 2014, 43, 402
    DOI: 10.1039/C3DT52848K

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