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Issue 17, 2014
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Synthesis of 6-acyl phenanthridines by oxidative radical decarboxylation–cyclization of α-oxocarboxylates and isocyanides

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Abstract

A silver catalysed synthesis of 6-acyl phenanthridines by oxidative radical decarboxylation–cyclization of α-oxocarboxylates and isocyanides was developed. This reaction provided a novel method to realize C1 insertion via a radical process and various functional groups were well-tolerated.

Graphical abstract: Synthesis of 6-acyl phenanthridines by oxidative radical decarboxylation–cyclization of α-oxocarboxylates and isocyanides

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Publication details

The article was received on 26 Nov 2013, accepted on 26 Dec 2013 and first published on 06 Jan 2014


Article type: Communication
DOI: 10.1039/C3CC49026B
Citation: Chem. Commun., 2014,50, 2145-2147
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    Synthesis of 6-acyl phenanthridines by oxidative radical decarboxylation–cyclization of α-oxocarboxylates and isocyanides

    J. Liu, C. Fan, H. Yin, C. Qin, G. Zhang, X. Zhang, H. Yi and A. Lei, Chem. Commun., 2014, 50, 2145
    DOI: 10.1039/C3CC49026B

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