Beijing National Laboratory for Molecular Sciences, Key Laboratory of Molecular Recognition and Function, Institute of Chemistry, Chinese Academy of Sciences, Beijing 100190, China
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Org. Biomol. Chem., 2013,11, 5722-5726
22 Apr 2013,
09 Jul 2013
First published online
10 Jul 2013
An unprecedented N-heterocyclic carbene (NHC) catalyzed Morita–Baylis–Hillman (MBH) reaction of β-substituted nitroalkenes and azodicarboxylates has been developed. Both β-aryl and β-alkyl nitroalkenes worked well for the reaction using 5 mol% of NHC catalyst, giving the desired α-hydrazino-α,β-unsaturated nitroalkenes in good to excellent yields.
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Organic & Biomolecular Chemistry
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