Issue 10, 2013
From the journal:

Organic & Biomolecular Chemistry

Tetrabutylammonium iodide catalyzed allylic sulfonylation of Baylis–Hillman acetates with sulfonylhydrazides in water†

Xiaoqing Li,*a   Xiangsheng Xu*a  and  Yucai Tanga  

* Corresponding authors

a College of Chemical Engineering and Materials Science, Zhejiang University of Technology, Hangzhou 310014, P. R. China
E-mail: xqli@zjut.edu.cn, future@zjut.edu.cn
Fax: +86 571 88320799
Tel: +86 571 88320799

Abstract

A tetrabutylammonium iodide catalyzed method for the synthesis of allyl aryl sulfone derivatives with Baylis–Hillman acetates and sulfonylhydrazides using tert-butyl hydroperoxide as an oxidation agent in water has been developed. In this process, the group eliminated from the sulfonyl precursor is molecular nitrogen.

Graphical abstract: Tetrabutylammonium iodide catalyzed allylic sulfonylation of Baylis–Hillman acetates with sulfonylhydrazides in water

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Article information

DOI
https://doi.org/10.1039/C3OB27329F
Article type
Paper
Submitted
30 Nov 2012
Accepted
18 Jan 2013
First published
22 Jan 2013

Org. Biomol. Chem., 2013,11, 1739-1742

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Tetrabutylammonium iodide catalyzed allylic sulfonylation of Baylis–Hillman acetates with sulfonylhydrazides in water

X. Li, X. Xu and Y. Tang, Org. Biomol. Chem., 2013, 11, 1739 DOI: 10.1039/C3OB27329F

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