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Department of Chemistry, Analytical and Biological Chemistry Research Facility, University College Cork, Ireland
Department of Chemistry and School of Pharmacy, Analytical and Biological Chemistry Research Facility, University College Cork, Ireland
; Fax: +353(0)214274097
; Tel: +353(0)214901694
Org. Biomol. Chem., 2013,11, 1706-1725
06 Jul 2012,
09 Jan 2013
First published online
10 Jan 2013
Diazo transfer adjacent to a sulfoxide moiety to provide stable, isolable α-diazo-β-oxo sulfoxides has been achieved. Use of monocyclic and bicyclic sulfoxide precursors is critical in enabling isolation of stable derivatives, through introduction of conformational constraint, while acyclic α-diazo-β-oxo sulfoxides are too labile to isolate and characterize.
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Organic & Biomolecular Chemistry
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