Nanostructural transformations during the reduction of hollow and porous nickel oxide nanoparticles

John A. Medford; Aaron C. Johnston-Peck; Joseph B. Tracy

doi:10.1039/C2NR33005A

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Nanoscale

Issue 1, 2013

A new peer reviewed journal publishing experimental and theoretical work across the breadth of nanoscience and nanotechnology

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Nanostructural transformations during the reduction of hollow and porous nickel oxide nanoparticles

John A. Medford,^a Aaron C. Johnston-Peck^a and Joseph B. Tracy*^a

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Department of Materials Science and Engineering, North Carolina State University, Raleigh, USA
E-mail: jbtracy@ncsu.edu

Nanoscale, 2013,5, 155-159

DOI: 10.1039/C2NR33005A
Received 02 Oct 2012, Accepted 01 Nov 2012
First published online 20 Nov 2012

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Size-dependent nanostructural transformations occurring during the H₂-mediated reduction of hollow and porous NiO nanoparticles were investigated for controlled nanoparticle sizes of [similar] 10 to 100 nm. Transmission electron microscopy reveals that the location and number of reduction sites strongly depend on the nanoparticle size and structure.