Catalytic isomerization of allylic alcohols in water by [RuClCp(PTA)2], [RuClCp(HPTA)2]Cl2·2H2O, [RuCp(DMSO-κS)(PTA)2]Cl, [RuCp(DMSO-κS)(PTA)2](OSO2CF3) and [RuCp(DMSO-κS)(HPTA)2]Cl3·2H2O

Manuel Serrano-Ruiz; Pablo Lorenzo-Luis; Antonio Romerosa; Adrian Mena-Cruz

doi:10.1039/C3DT32998D

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Dalton Transactions

Issue 21, 2013

The international journal for inorganic, organometallic and bioinorganic chemistry

Impact Factor 3.838 48 Issues per Year Indexed in MEDLINE

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Catalytic isomerization of allylic alcohols in water by [RuClCp(PTA)₂], [RuClCp(HPTA)₂]Cl₂·2H₂O, [RuCp(DMSO-κS)(PTA)₂]Cl, [RuCp(DMSO-κS)(PTA)₂](OSO₂CF₃) and [RuCp(DMSO-κS)(HPTA)₂]Cl₃·2H₂O

Manuel Serrano-Ruiz,^a Pablo Lorenzo-Luis,^b Antonio Romerosa*^a and Adrian Mena-Cruz^b

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Área de Química Inorgánica, Facultad de Ciencias, Universidad de Almería, Almería, Spain
E-mail: romerosa@ual.es ;
Fax: +34 950015008

Departamento de Química Inorgánica, Facultad de Química, Universidad de La Laguna, La Laguna, Spain

Dalton Trans., 2013,42, 7622-7630

DOI: 10.1039/C3DT32998D
Received 13 Dec 2012, Accepted 23 Feb 2013
First published online 26 Feb 2013

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The new water soluble complexes [RuClCp(HPTA)₂]Cl₂·2H₂O (2), [RuCp(DMSO-κS)(PTA)₂]Cl (3), [RuCp(DMSO-κS)(PTA)₂](OSO₂CF₃) (4) and [RuCp(DMSO-κS)(HPTA)₂]Cl₃·2H₂O (5) have been synthesized and fully characterized by NMR, IR and elemental analysis. The structures of complexes 2·2H₂O and 5·2H₂O were also characterized by single crystal X-ray determination. The catalytic activity of the complexes and [RuClCp(PTA)₂] (1) for the isomerisation in water of 1-octen- to 1-penten-3-ol was assessed and discussed.

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Dalton Transactions

Catalytic isomerization of allylic alcohols in water by [RuClCp(PTA)₂], [RuClCp(HPTA)₂]Cl₂·2H₂O, [RuCp(DMSO-κS)(PTA)₂]Cl, [RuCp(DMSO-κS)(PTA)₂](OSO₂CF₃) and [RuCp(DMSO-κS)(HPTA)₂]Cl₃·2H₂O

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Dalton Transactions

Catalytic isomerization of allylic alcohols in water by [RuClCp(PTA)2], [RuClCp(HPTA)2]Cl2·2H2O, [RuCp(DMSO-κS)(PTA)2]Cl, [RuCp(DMSO-κS)(PTA)2](OSO2CF3) and [RuCp(DMSO-κS)(HPTA)2]Cl3·2H2O

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Catalytic isomerization of allylic alcohols in water by [RuClCp(PTA)₂], [RuClCp(HPTA)₂]Cl₂·2H₂O, [RuCp(DMSO-κS)(PTA)₂]Cl, [RuCp(DMSO-κS)(PTA)₂](OSO₂CF₃) and [RuCp(DMSO-κS)(HPTA)₂]Cl₃·2H₂O