Crystal structure and magnetic properties of Pb2Ni(PO4)2

Zhangzhen He; Weilong Zhang; Tianlong Xia; Weiqiang Yu; Wendan Cheng

doi:10.1039/C3DT00030C

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Dalton Transactions

Issue 15, 2013

The international journal for inorganic, organometallic and bioinorganic chemistry

Impact Factor 3.838 48 Issues per Year Indexed in MEDLINE

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Paper

Crystal structure and magnetic properties of Pb₂Ni(PO₄)₂

Zhangzhen He,*^a Weilong Zhang,^a Tianlong Xia,^b Weiqiang Yu^b and Wendan Cheng^a

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Corresponding authors

State Key Laboratory of Structural Chemistry, Fujian Institute of Research on the Structure of Mater, Chinese Academy of Sciences, Fuzhou, China
E-mail: hezz@fjirsm.ac.cn

Department of Physics, Renmin University of China, Beijing 100872, China

Dalton Trans., 2013,42, 5480-5484

DOI: 10.1039/C3DT00030C
Received 27 Jun 2012, Accepted 04 Jan 2013
First published online 01 Feb 2013

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Abstract
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A new NiO-based material Pb₂Ni(PO₄)₂ was obtained by a conventional solid-state reaction in air. The crystal structure exhibits both corner- and edge-sharing {Ni–O–P} bonds in the system. Magnetic properties were investigated by means of magnetic susceptibility, magnetization, and heat capacity measurements. The results show a typical three-dimensional antiferromagnetic ordering below [similar] 4 K and a field-induced spin-flop transition below the Néel temperature.