A cyclopalladated complex of corannulene with a pyridine pendant and its columnar self-assembly

Mihoko Yamada; Shohei Tashiro; Ryosuke Miyake; Mitsuhiko Shionoya

doi:10.1039/C2DT32883F

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Dalton Transactions

Issue 10, 2013

The international journal for inorganic, organometallic and bioinorganic chemistry

Impact Factor 3.838 48 Issues per Year Indexed in MEDLINE

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A cyclopalladated complex of corannulene with a pyridine pendant and its columnar self-assembly

Mihoko Yamada,^a Shohei Tashiro,^a Ryosuke Miyake^b and Mitsuhiko Shionoya*^a

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Department of Chemistry, Graduate School of Science, The University of Tokyo, 7-3-1 Hongo, Bunkyo-ku, Tokyo 113-0033, Japan
E-mail: shionoya@chem.s.u-tokyo.ac.jp ;
Fax: +81 03 5841 8061 ;
Tel: +81 03 5841 8061

Department of Chemistry and Biochemistry, Graduate School of Humanities and Science, Ochanomizu University, 2-1-1 Otsuka, Bunkyo-ku, Tokyo 112-8610, Japan

Dalton Trans., 2013,42, 3300-3303

DOI: 10.1039/C2DT32883F
Received 01 Dec 2012, Accepted 04 Jan 2013
First published online 07 Jan 2013

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Abstract
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Bowl-shaped corannulene provides various metal binding modes with its curved π-surfaces and rim. Herein, we report the syntheses of 2-pyridylcorannulene and its cyclopalladated complex. Its expanded π-system and columnar self-assembly in the crystal state were revealed by NMR and UV-vis spectroscopies, ESI-TOF mass spectrometry and single-crystal X-ray analysis.

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A cyclopalladated complex of corannulene with a pyridine pendant and its columnar self-assembly

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