Hydrothermal synthesis of an ortho-metallated Co(III) complex anchored by a carboxylate group with a selective oxidation catalytic property

Shi-Yuan Zhang; Wei Shi; Jian-Gong Ma; Yu-Qi Zhang; Zhen-Jie Zhang; Peng Cheng

doi:10.1039/C2DT32468G

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Dalton Transactions

Issue 12, 2013

The international journal for inorganic, organometallic and bioinorganic chemistry

Impact Factor 3.838 48 Issues per Year Indexed in MEDLINE

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Hydrothermal synthesis of an ortho-metallated Co(III) complex anchored by a carboxylate group with a selective oxidation catalytic property

Shi-Yuan Zhang,^a Wei Shi,*^a Jian-Gong Ma,^a Yu-Qi Zhang,^a Zhen-Jie Zhang^a and Peng Cheng*^a

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Department of Chemistry and Key Laboratory of Advanced Energy Materials Chemistry (MOE), TKL of Metal and Molecule Based Material Chemistry, Nankai University, Tianjin 300071, P. R. China
E-mail: shiwei@nankai.edu.cn ;
Fax: +86-022-23502458 ;
Tel: +86-022-23503059

Dalton Trans., 2013,42, 4313-4318

DOI: 10.1039/C2DT32468G
Received 17 Oct 2012, Accepted 17 Dec 2012
First published online 17 Dec 2012

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Abstract
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An air-stable and water-tolerant ortho-metallated complex [Co(tfb)(bpy)₂](NO₃)·3H₂O was obtained via hydrothermal synthesis. The mechanism for the formation of Co–C bond was studied using both DFT calculations and experimental analysis. This highly stable complex exhibits good catalytic performance for the selective oxidation of cyclohexane.

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Shi-Yuan Zhang
Wei Shi
Jian-Gong Ma
Yu-Qi Zhang
Zhen-Jie Zhang
Peng Cheng

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