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Issue 59, 2013
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Signal enhancement of J-HMQC experiments in solid-state NMR involving half-integer quadrupolar nuclei

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Abstract

We show that for half-integer quadrupolar nuclei, the manipulation of the satellite transitions can accelerate and enhance coherence transfer to other isotopes. This novel strategy is demonstrated to improve the sensitivity of 31P-{27Al} J-HMQC experiments for a layered aluminophosphate Mu-4.

Graphical abstract: Signal enhancement of J-HMQC experiments in solid-state NMR involving half-integer quadrupolar nuclei

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Publication details

The article was received on 22 Apr 2013, accepted on 03 Jun 2013 and first published on 04 Jun 2013


Article type: Communication
DOI: 10.1039/C3CC42961J
Citation: Chem. Commun., 2013,49, 6653-6655
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    Signal enhancement of J-HMQC experiments in solid-state NMR involving half-integer quadrupolar nuclei

    Q. Wang, J. Trébosc, Y. Li, J. Xu, B. Hu, N. Feng, Q. Chen, O. Lafon, J. Amoureux and F. Deng, Chem. Commun., 2013, 49, 6653
    DOI: 10.1039/C3CC42961J

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