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Issue 26, 2013
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One-pot synthesis of benzamide over a robust tandem catalyst based on center radially fibrous silica encapsulated TS-1

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Abstract

A center radially fibrous silica encapsulated TS-1 zeolite (TS-1@KCC-1) has been synthesized in a microemulsion system for the first time. Supporting the Rh(OH)3 species, this novel core–shell structured material serves as a robust bifunctional catalyst for one-pot synthesis of benzamide from benzaldehyde, ammonia and hydrogen peroxide, in which the aldehyde ammoximation and oxime rearrangement occur in a tandem way.

Graphical abstract: One-pot synthesis of benzamide over a robust tandem catalyst based on center radially fibrous silica encapsulated TS-1

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Publication details

The article was received on 28 Nov 2012, accepted on 07 Feb 2013 and first published on 08 Feb 2013


Article type: Communication
DOI: 10.1039/C3CC38546A
Citation: Chem. Commun., 2013,49, 2709-2711
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    One-pot synthesis of benzamide over a robust tandem catalyst based on center radially fibrous silica encapsulated TS-1

    H. Peng, L. Xu, H. Wu, K. Zhang and P. Wu, Chem. Commun., 2013, 49, 2709
    DOI: 10.1039/C3CC38546A

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