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Issue 80, 2013
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Unprecedented ortho-acylation of azoxybenzenes with α-oxocarboxylic acids by Pd-catalyzed C–H activation and decarboxylation

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Abstract

A palladium-catalyzed ortho-acylation reaction of azoxybenzenes with α-oxocarboxylic acids was developed in the presence of K2S2O8. The established methodology provides a direct approach to obtain acylated azoxybenzenes in good yields.

Graphical abstract: Unprecedented ortho-acylation of azoxybenzenes with α-oxocarboxylic acids by Pd-catalyzed C–H activation and decarboxylation

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Publication details

The article was received on 19 Jul 2013, accepted on 05 Aug 2013 and first published on 08 Aug 2013


Article type: Communication
DOI: 10.1039/C3CC45492D
Citation: Chem. Commun., 2013,49, 9170-9172
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    Unprecedented ortho-acylation of azoxybenzenes with α-oxocarboxylic acids by Pd-catalyzed C–H activation and decarboxylation

    H. Li, P. Li, Q. Zhao and L. Wang, Chem. Commun., 2013, 49, 9170
    DOI: 10.1039/C3CC45492D

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