Freeze-drying yields stable and pure amorphous calcium carbonate (ACC)

Johannes Ihli; Alexander N. Kulak; Fiona C. Meldrum

doi:10.1039/C3CC40807H

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Chemical Communications

Issue 30, 2013

Urgent high quality communications from across the chemical sciences.

Impact Factor 6.169 100 Issues per Year Indexed in MEDLINE

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Freeze-drying yields stable and pure amorphous calcium carbonate (ACC)

Johannes Ihli,*^a Alexander N. Kulak^a and Fiona C. Meldrum*^a

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School of Chemistry, University of Leeds, Leeds, UK
E-mail: F.Meldrum@leeds.ac.uk ;
Fax: +44 (0)113 343 6565 ;
Tel: +44 (0)113 343 6414

Chem. Commun., 2013,49, 3134-3136

DOI: 10.1039/C3CC40807H
Received 30 Jan 2013, Accepted 26 Feb 2013
First published online 26 Feb 2013

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A simple synthetic method is presented for the precipitation of high purity, dry amorphous calcium carbonate (ACC) based on freeze-drying saturated, counter ion free CaCO₃ solutions, where the ACC produced shows an extended atmospheric stability. Translation of the methodology to amorphous calcium phosphate demonstrates the generality of the approach.

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