Stepwise ligand transformations through [2+2] photodimerization and hydrothermal in situ oxidation reactions

Dong Liu; Jian-Ping Lang; Brendan F. Abrahams

doi:10.1039/C3CC39286D

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Chemical Communications

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Stepwise ligand transformations through [2+2] photodimerization and hydrothermal in situ oxidation reactions

Dong Liu,^a^b Jian-Ping Lang*^a and Brendan F. Abrahams^c

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College of Chemistry, Chemical Engineering and Materials Science, Soochow University, 199 RenAi Road, Suzhou 215123, P. R. China
E-mail: jplang@suda.edu.cn ;
Fax: +86 512 65880089 ;
Tel: +86 512 65882865

College of Chemistry and Materials Science, Huaibei Normal University, Huaibei 235000, P. R. China

School of Chemistry, University of Melbourne, Australia

Chem. Commun., 2013,49, 2682-2684

DOI: 10.1039/C3CC39286D
Received 30 Dec 2012, Accepted 12 Feb 2013
First published online 14 Feb 2013

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The SCSC transformation of a 1D polymer [Cd(1,3-bdc)(4-spy)₂]_n produced a 2D polymer [Cd(1,3-bdc)(4-spy)(HT-ppcb)_0.5]_n through the [2+2] photodimerization reaction. Hydrothermal reactions of HT-ppcb with CdCl₂, 1,3-H₂bdc and H₂O₂ afforded another 2D polymer {[Cd(H₂O)(1,3-bdc)(bpbpf)]·H₂O}_n in which HT-ppcb underwent in situ oxidation to form a unique furan-based ligand bpbpf.

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