Enantioselective synthesis of 1,2,4-triazolines by chiral iron(II)-complex catalyzed cyclization of α-isocyano esters and azodicarboxylates

Min Wang; Xiaohua Liu; Peng He; Lili Lin; Xiaoming Feng

doi:10.1039/C3CC39088H

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Chemical Communications

Issue 25, 2013

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Enantioselective synthesis of 1,2,4-triazolines by chiral iron(II)-complex catalyzed cyclization of α-isocyano esters and azodicarboxylates

Min Wang,^a Xiaohua Liu,*^a Peng He,^a Lili Lin^a and Xiaoming Feng*^a

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Key Laboratory of Green Chemistry & Technology, Ministry of Education, College of Chemistry, Sichuan University, Chengdu 610064, P. R. China
E-mail: xmfeng@scu.edu.cn ;
Fax: +86 28 85418249 ;
Tel: +86 28 85418249

Chem. Commun., 2013,49, 2572-2574

DOI: 10.1039/C3CC39088H
Received 20 Dec 2012, Accepted 05 Feb 2013
First published online 20 Feb 2013

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Enantioselective cyclization of α-isocyano esters with azodicarboxylates catalyzed by Fe^II–N,N′-dioxide complexes has been developed. Under mild conditions, a variety of 1,2,4-triazoline derivatives was obtained in high yields and enantioselectivities.

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Min Wang
Xiaohua Liu
Peng He
Lili Lin
Xiaoming Feng

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Enantioselective synthesis of 1,2,4-triazolines by chiral iron(II)-complex catalyzed cyclization of α-isocyano esters and azodicarboxylates

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Enantioselective synthesis of 1,2,4-triazolines by chiral iron(II)-complex catalyzed cyclization of α-isocyano esters and azodicarboxylates

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