P–P bond formation via reductive dimerization of [Cp*Fe(η5-P5)] by divalent samarocenes

Tianshu Li; Michael T. Gamer; Manfred Scheer; Sergey N. Konchenko; Peter W. Roesky

doi:10.1039/C3CC38841G

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Chemical Communications

Issue 22, 2013

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P–P bond formation via reductive dimerization of [Cp*Fe(η⁵-P₅)] by divalent samarocenes

Tianshu Li,^a Michael T. Gamer,^a Manfred Scheer,^b Sergey N. Konchenko*^a^c and Peter W. Roesky*^a

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Institut für Anorganische Chemie, Karlsruher Institut für Technologie (KIT), Engesserstr. 15, Geb. 30.45, 76131 Karlsruhe, Germany
E-mail: roesky@kit.edu

Institut für Anorganische Chemie der Universität Regensburg, 93040 Regensburg, Germany

Nikolaev Institute of Inorganic Chemistry SB RAS, Prosp. Lavrentieva 3, 630090 Novosibirsk, Russia

Chem. Commun., 2013,49, 2183-2185

DOI: 10.1039/C3CC38841G
Received 10 Dec 2012, Accepted 18 Jan 2013
First published online 05 Feb 2013

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Abstract
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The two new 3d/4f polyphosphide complexes [(Cp*Fe)₂P₁₀{Sm(η⁵-C₅Me₄R)₂}₂] (Cp* = η⁵-C₅Me₅; R = Me, nPr) were prepared by reductive dimerization of [Cp*Fe(η⁵-P₅)] with samarocenes. They are the first P₁₀ bridging 3d/4f metal complexes and the first examples of reductive coupling of polyphosphide complexes by divalent lanthanides.

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Tianshu Li
Michael T. Gamer
Manfred Scheer
Sergey N. Konchenko
Peter W. Roesky

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Chemical Communications

P–P bond formation via reductive dimerization of [Cp*Fe(η⁵-P₅)] by divalent samarocenes

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P–P bond formation via reductive dimerization of [Cp*Fe(η5-P5)] by divalent samarocenes

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P–P bond formation via reductive dimerization of [Cp*Fe(η⁵-P₅)] by divalent samarocenes