Spin-active metallofullerene stabilized by the core of an NC moiety

Yongqiang Feng; Taishan Wang; Jingyi Wu; Yihan Ma; Zhuxia Zhang; Li Jiang; Chunhua Ge; Chunying Shu; Chunru Wang

doi:10.1039/C3CC38445D

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Chemical Communications

Issue 21, 2013

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Spin-active metallofullerene stabilized by the core of an NC moiety

Yongqiang Feng,^a Taishan Wang,*^a Jingyi Wu,^b Yihan Ma,^a Zhuxia Zhang,^a Li Jiang,^a Chunhua Ge,*^c Chunying Shu^a and Chunru Wang*^a

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Key Laboratory of Molecular Nanostructure and Nanotechnology, Beijing National Laboratory for Molecular Sciences, Institute of Chemistry, Chinese Academy of Sciences, Beijing, China
E-mail: wangtais@iccas.ac.cn ;
Tel: +86-10-62652120

Laboratory of Nuclear Analysis Techniques, Institute of High Energy Physics, Chinese Academy of Sciences, Beijing, China

College of Chemistry, Liaoning University, Shenyang, China
E-mail: chhge@lnu.edu.cn ;
Tel: +86-24-62202550

Chem. Commun., 2013,49, 2148-2150

DOI: 10.1039/C3CC38445D
Received 23 Nov 2012, Accepted 30 Jan 2013
First published online 30 Jan 2013

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A paramagnetic Sc₃NC@C₈₀ anion radical was obtained by chemical reduction. ESR spectrometry and theoretical calculations disclosed that the core NC moiety takes possession of the unpaired electron and stabilizes the paramagnetic species. It is the first time a paramagnetic metal cyanide metallofullerene has been obtained.

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Yongqiang Feng
Taishan Wang
Jingyi Wu
Yihan Ma
Zhuxia Zhang
Li Jiang
Chunhua Ge
Chunying Shu
Chunru Wang

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