Iodine-catalyzed tandem synthesis of terminal acetals and glycol mono esters from olefins

Macharla Arun Kumar; Peraka Swamy; Mameda Naresh; Marri Mahender Reddy; Chozhiyath Nappunni Rohitha; Sripadi Prabhakar; Akella Venkata Subrahmanya Sarma; Joseph Richard Prem Kumar; Nama Narender

doi:10.1039/C3CC38085H

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Chemical Communications

Issue 17, 2013

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Iodine-catalyzed tandem synthesis of terminal acetals and glycol mono esters from olefins

Macharla Arun Kumar,^a Peraka Swamy,^a Mameda Naresh,^a Marri Mahender Reddy,^a Chozhiyath Nappunni Rohitha,^a Sripadi Prabhakar,^b Akella Venkata Subrahmanya Sarma,^c Joseph Richard Prem Kumar^d and Nama Narender*^a

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I&PC Division, CSIR-IICT, Hyderabad 500 007, India
E-mail: narendern33@yahoo.co.in

NCMS, CSIR-IICT, Hyderabad 500 007, India

Centre for NMR, CSIR-IICT, Hyderabad 500 007, India

CMM, CSIR-IICT, Hyderabad 500 007, India

Chem. Commun., 2013,49, 1711-1713

DOI: 10.1039/C3CC38085H
Received 08 Nov 2012, Accepted 09 Jan 2013
First published online 11 Jan 2013

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A new metal-free protocol is described for the synthesis of terminal acetals by tandem oxidative rearrangement of olefins using oxone as an oxidant in the presence of iodine. Moreover, a one-pot procedure for the preparation of glycol mono esters from olefins is also presented for the first time using the same reagent system.

Abstract from Methods in Organic Synthesis 2013

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Macharla Arun Kumar
Peraka Swamy
Mameda Naresh
Marri Mahender Reddy
Chozhiyath Nappunni Rohitha
Sripadi Prabhakar
Akella Venkata Subrahmanya Sarma
Joseph Richard Prem Kumar
Nama Narender

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Chemical Communications

Iodine-catalyzed tandem synthesis of terminal acetals and glycol mono esters from olefins

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Chemical Communications

Iodine-catalyzed tandem synthesis of terminal acetals and glycol mono esters from olefins

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