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Reaction of oxabicyclic alkenes with alkynes and organoboronic acids in the presence of Ni(cod)2, P(t-Bu)3, and CsF in a binary solvent toluene–methanol (1:3) at 75 to 85 °C provided exo-5,6-disubstituted 7-oxanorbornene derivatives in good to excellent yields.
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