Bridging π-coordination of pyrrole and indole over a PdI–PdI bond

Tetsuro Murahashi; Seita Kimura; Kohei Takase; Sensuke Ogoshi; Koji Yamamoto

doi:10.1039/C2CC37554K

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Chemical Communications

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Bridging π-coordination of pyrrole and indole over a Pd^I–Pd^I bond

Tetsuro Murahashi,*^a^b Seita Kimura,^a^c Kohei Takase,^c Sensuke Ogoshi^c and Koji Yamamoto^a

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Institute for Molecular Science, Myodaiji, Okazaki, Japan
E-mail: mura@ims.ac.jp ;
Fax: +81-564-59-5582

PRESTO, Japan Science and Technology Agency (JST), Japan

Department of Applied Chemistry, Graduate School of Engineering, Osaka University, Suita, Japan

Chem. Commun., 2013,49, 4310-4312

DOI: 10.1039/C2CC37554K
Received 17 Oct 2012, Accepted 03 Dec 2012
First published online 20 Dec 2012

This article is part of themed collection: Emerging Investigators 2013

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Abstract
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π-Coordination of pyrrole or indole which lack a chelating functionality to a dinuclear Pd^I–Pd^I center is revealed. The dinuclear sandwich Pd^I–Pd^I complexes of pyrrole, N-methylpyrrole, or indole were synthesized and structurally characterized by X-ray crystallographic analysis. Indole employs the carbons of the six-membered ring in bridging π-coordination to a Pd^I–Pd^I center.

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Tetsuro Murahashi
Seita Kimura
Kohei Takase
Sensuke Ogoshi
Koji Yamamoto

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