A highly regioselective sp3 C–H amination of tertiary amides based on Fe(II) complex catalysts

Xuerong Mao; Yuanzhao Wu; Xiaoxiang Jiang; Xunhua Liu; Yixiang Cheng; Chengjian Zhu

doi:10.1039/C2RA20707A

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RSC Advances

Issue 17, 2012

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A highly regioselective sp³ C–H amination of tertiary amides based on Fe(II) complex catalysts

Xuerong Mao,^a Yuanzhao Wu,^a Xiaoxiang Jiang,^a Xunhua Liu,^a Yixiang Cheng*^a and Chengjian Zhu*^a

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Key Lab of Mesoscopic Chemistry of MOE, School of Chemistry and Chemical Engineering, Nanjing University, China
E-mail: yxcheng@nju.edu.cn, ;
Fax: +86-25-88317761 ;
Tel: +86-25-83686508

RSC Adv., 2012,2, 6733-6735

DOI: 10.1039/C2RA20707A
Received 18 Apr 2012, Accepted 14 May 2012
First published online 16 May 2012

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A highly regioselective sp³ C–H amination of aryl amides with N-substituted pyrrolidin-2-ones has been developed with a catalyst Fe(II) complex with TBHP as a benign oxidant. This facile method can offer rapid access to the amination reaction of N-substituted pyrrolidin-2-ones in moderate to excellent yields.

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Xuerong Mao
Yuanzhao Wu
Xiaoxiang Jiang
Xunhua Liu
Yixiang Cheng
Chengjian Zhu

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