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Issue 27, 2012
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Continuous-flow synthesis of activated vitamin D3 and its analogues

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Abstract

An efficient, two-stage, continuous-flow synthesis of 1α,25-(OH)2-vitamin D3 (activated vitamin D3) and its analogues was achieved. The developed method afforded the desired products in satisfactory yields using a high-intensity and economical light source, i.e., a high-pressure mercury lamp. In addition, our method required neither intermediate purification nor high-dilution conditions.

Graphical abstract: Continuous-flow synthesis of activated vitamin D3 and its analogues

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Publication details

The article was received on 09 Mar 2012, accepted on 24 Apr 2012 and first published on 25 Apr 2012


Article type: Paper
DOI: 10.1039/C2OB25511A
Citation: Org. Biomol. Chem., 2012,10, 5205-5211
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    Continuous-flow synthesis of activated vitamin D3 and its analogues

    S. Fuse, Y. Mifune, N. Tanabe and T. Takahashi, Org. Biomol. Chem., 2012, 10, 5205
    DOI: 10.1039/C2OB25511A

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