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School of Biological and Chemical Sciences, Queen Mary University of London, Joseph Priestley Building, Mile End Road, E1 4NS, London, UK
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Org. Biomol. Chem., 2012,10, 3172-3174
19 Jan 2012,
01 Mar 2012
First published online
05 Mar 2012
A practical, mild and highly selective protocol for the monodeuteration of a variety of arenes and heteroarenes is presented. Catalytic amounts of Ag(I) salts in DMSO/D2O are shown to facilitate the deutero-decarboxylation of ortho-substituted benzoic and heteroaromatic α-carboxylic acids in high yields with excellent levels of deuterium incorporation.
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Organic & Biomolecular Chemistry
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