Hydrogenation of imines catalysed by ruthenium(II) complexes based on lutidine-derived CNC pincer ligands

Martín Hernández-Juárez; Mónica Vaquero; Eleuterio Álvarez; Verónica Salazar; Andrés Suárez

doi:10.1039/C2DT31907A

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Dalton Transactions

Issue 2, 2013

The international journal for inorganic, organometallic and bioinorganic chemistry

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Hydrogenation of imines catalysed by ruthenium(II) complexes based on lutidine-derived CNC pincer ligands

Martín Hernández-Juárez,^a Mónica Vaquero,^b Eleuterio Álvarez,^b Verónica Salazar*^a and Andrés Suárez*^b

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Centro de Investigaciones Químicas, Universidad Autónoma del Estado de Hidalgo, Carretera Pachuca-Tulancingo Km 4.5, 42184, Mineral de la Reforma, Hidalgo, Mexico
E-mail: salazar@uaeh.edu.mx ;
Fax: +52 771 717200x6502 ;
Tel: +52 771 1550933

Instituto de Investigaciones Químicas (IIQ), Consejo Superior de Investigaciones Científicas and Universidad de Sevilla, Avda Américo Vespucio No. 49, 41092, Sevilla, Spain
E-mail: andres.suarez@iiq.csic.es ;
Fax: +34954460565 ;
Tel: +34 954489556

Dalton Trans., 2013,42, 351-354

DOI: 10.1039/C2DT31907A
Received 20 Aug 2012, Accepted 26 Sep 2012
First published online 03 Oct 2012

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Abstract
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The preparation of new Ru(II) complexes incorporating fac-coordinated lutidine-derived CNC ligands is reported. These derivatives are selectively deprotonated by ^tBuOK at one of the methylene arms of the pincer, leading to catalytically active species in the hydrogenation of imines.

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Martín Hernández-Juárez
Mónica Vaquero
Eleuterio Álvarez
Verónica Salazar
Andrés Suárez

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