Trapping {BW12}2 tungstoborate: synthesis and crystal structure of hybrid [{(H2BW12O42)2O}{Mo6O6S6(OH)4(H2O)2}]14− anion

V. S. Korenev; P. A. Abramov; C. Vicent; D. A. Mainichev; S. Floquet; E. Cadot; M. N. Sokolov; V. P. Fedin

doi:10.1039/C2DT31512B

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Dalton Transactions

Issue 48, 2012

The international journal for inorganic, organometallic and bioinorganic chemistry

Impact Factor 3.838 48 Issues per Year Indexed in MEDLINE

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Trapping {BW₁₂}₂ tungstoborate: synthesis and crystal structure of hybrid [{(H₂BW₁₂O₄₂)₂O}{Mo₆O₆S₆(OH)₄(H₂O)₂}]¹⁴⁻ anion

V. S. Korenev,*^a^b^d P. A. Abramov,^a^d C. Vicent,^c D. A. Mainichev,^a S. Floquet,^b E. Cadot,*^b M. N. Sokolov^a^d and V. P. Fedin^a^d

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Nikolaev Institute of Inorganic Chemistry SB RAS, Prospect Lavrentyeva 3, 630090 Novosibirsk, Russia
E-mail: wkorenev@niic.nsc.ru ;
Fax: +7 383 330 9089 ;
Tel: +7 383 316 5845

Institut Lavoisier de Versailles, Université de Versailles Saint Quentin, UMR 8180, 45 avenue des Etats Unis, 78035 Versailles, France
E-mail: cadot@chimie.uvsq.fr ;
Fax: +33 01 39 25 44 52 ;
Tel: +33 01 39 25 43 82

Universitat Jaume I CIF: Q-6250003-H, Av. de Vicent Sos Baynat, s/n, 12071 Castelló de la Plana, Espanya ;
Fax: +34 964 72 90 16 ;
Tel: +34 964 72 80 00

Novosibirsk State Univeristy, Pirogova Str. 2, Novosibirsk, Russia

Dalton Trans., 2012,41, 14484-14486

DOI: 10.1039/C2DT31512B
Received 10 Jul 2012, Accepted 17 Aug 2012
First published online 17 Aug 2012

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Abstract
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Reaction between monolacunary {BW₁₁} tungstoborate and oxothiocationic building block, {Mo₂O₂S₂}, results in the formation of a new polyoxothiometalate with a unique architecture in which two [H₂BW₁₂O₄₃]⁹⁻ tungstoborate subunits are linked together with a hexamolybdate [Mo^V₆O₆S₆(OH)₄(H₂O)₂]²⁺ bridge.

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V. S. Korenev
P. A. Abramov
C. Vicent
D. A. Mainichev
S. Floquet
E. Cadot
M. N. Sokolov
V. P. Fedin

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Dalton Transactions

Trapping {BW₁₂}₂ tungstoborate: synthesis and crystal structure of hybrid [{(H₂BW₁₂O₄₂)₂O}{Mo₆O₆S₆(OH)₄(H₂O)₂}]¹⁴⁻ anion

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Dalton Transactions

Trapping {BW12}2 tungstoborate: synthesis and crystal structure of hybrid [{(H2BW12O42)2O}{Mo6O6S6(OH)4(H2O)2}]14− anion

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Trapping {BW₁₂}₂ tungstoborate: synthesis and crystal structure of hybrid [{(H₂BW₁₂O₄₂)₂O}{Mo₆O₆S₆(OH)₄(H₂O)₂}]¹⁴⁻ anion