Facile formation of five-membered N-heterocyclic zirconacycloallenoids

Santhosh Kumar Podiyanachari; Roland Fröhlich; Constantin G. Daniliuc; Jeffrey L. Petersen; Gerald Kehr; Gerhard Erker; Noriyuki Suzuki; Shin Yuasa; Keita Hagimori; Shota Inoue; Takumi Asada; Takahiko Takemoto; Yoshiro Masuyama

doi:10.1039/C2DT31343J

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Dalton Transactions

Issue 35, 2012

The international journal for inorganic, organometallic and bioinorganic chemistry

Impact Factor 3.838 48 Issues per Year Indexed in MEDLINE

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Facile formation of five-membered N-heterocyclic zirconacycloallenoids

Santhosh Kumar Podiyanachari,^a Roland Fröhlich,^a Constantin G. Daniliuc,^a Jeffrey L. Petersen,^b Gerald Kehr,^a Gerhard Erker,*^a Noriyuki Suzuki,*^c Shin Yuasa,^c Keita Hagimori,^c Shota Inoue,^c Takumi Asada,^c Takahiko Takemoto^c and Yoshiro Masuyama^c

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Organisch-Chemisches Institut, Universität Münster, Corrensstrasse 40, D-48149 Münster, Germany
E-mail: erker@uni-muenster.de

Bennett Department of Chemistry, West Virginia University, P.O. Box 6045, Morgantown, USA

Department of Materials and Life Sciences, Faculty of Science and Technology, Sophia University, 7-1 Kioi-cho, Chiyoda-ku, Tokyo, Japan
E-mail: norisuzuki@sophia.ac.jp

Dalton Trans., 2012,41, 10811-10816

DOI: 10.1039/C2DT31343J
Received 22 Jun 2012, Accepted 18 Jul 2012
First published online 20 Jul 2012

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The reaction of η²-iminozirconocene chloride complexes with trimethylsilylethynyl lithium leads to rapid C–C coupling at room temperature to yield the corresponding five-membered aza-zirconacycloallenoids. Such compounds were also obtained by trapping of in situ generated zirconocene with alkynyl imines.

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Facile formation of five-membered N-heterocyclic zirconacycloallenoids

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