The formation and stability of molybdenum–antimony and tungsten–antimony ternary oxides Sb2MO6, Sb2M2O9, Sb2Mo3O12 and Sb4MO9 in the gas phase (M = Mo, W). Quantum chemical and mass spectrometric studies

E. Berezovskaya; E. Milke; M. Binnewies

doi:10.1039/C2DT31058A

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Dalton Transactions

Issue 35, 2012

The international journal for inorganic, organometallic and bioinorganic chemistry

Impact Factor 3.838 48 Issues per Year Indexed in MEDLINE

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The formation and stability of molybdenum–antimony and tungsten–antimony ternary oxides Sb₂MO₆, Sb₂M₂O₉, Sb₂Mo₃O₁₂ and Sb₄MO₉ in the gas phase (M = Mo, W). Quantum chemical and mass spectrometric studies

E. Berezovskaya,*^a E. Milke^a and M. Binnewies^a

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Institut für Anorganische Chemie, Leibniz Universität Hannover, Callinstr. 9, 30167 Hannover, Germany
E-mail: katja.berezovskaya@aca.uni-hannover.de ;
Fax: +49-0511-762-2254

Dalton Trans., 2012,41, 10769-10776

DOI: 10.1039/C2DT31058A
Received 16 May 2012, Accepted 06 Jul 2012
First published online 06 Jul 2012

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The ternary oxides Sb₂MO₆, Sb₂M₂O₉, Sb₄MO₉ (M = Mo, W) and Sb₂Mo₃O₁₂ were detected in the gas phase by means of mass spectrometry (MS). These gaseous oxides are reported for the first time. Thermodynamic data was obtained experimentally and confirmed by quantum chemical (QC) calculations. In addition, structural data on these molecules was obtained. The ionisation potentials (IP) were also determined both experimentally and theoretically.

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Dalton Transactions

The formation and stability of molybdenum–antimony and tungsten–antimony ternary oxides Sb₂MO₆, Sb₂M₂O₉, Sb₂Mo₃O₁₂ and Sb₄MO₉ in the gas phase (M = Mo, W). Quantum chemical and mass spectrometric studies

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Dalton Transactions

The formation and stability of molybdenum–antimony and tungsten–antimony ternary oxides Sb2MO6, Sb2M2O9, Sb2Mo3O12 and Sb4MO9 in the gas phase (M = Mo, W). Quantum chemical and mass spectrometric studies

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The formation and stability of molybdenum–antimony and tungsten–antimony ternary oxides Sb₂MO₆, Sb₂M₂O₉, Sb₂Mo₃O₁₂ and Sb₄MO₉ in the gas phase (M = Mo, W). Quantum chemical and mass spectrometric studies