A fluorophosphate-based inverse Keggin structure

John Fielden; Kyle Quasdorf; Leroy Cronin; Paul Kögerler

doi:10.1039/C2DT30501A

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Dalton Transactions

Issue 33, 2012

The international journal for inorganic, organometallic and bioinorganic chemistry

Impact Factor 3.838 48 Issues per Year Indexed in MEDLINE

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A fluorophosphate-based inverse Keggin structure

John Fielden,^a^b Kyle Quasdorf,^a Leroy Cronin^c and Paul Kögerler*^a^b

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Ames Laboratory, Iowa State University, Ames, USA

Institute of Inorganic Chemistry, RWTH Aachen University, 52074 Aachen, Germany
E-mail: paul.koegerler@ac.rwth-aachen.de

WestCHEM, University of Glasgow, Glasgow, UK

Dalton Trans., 2012,41, 9876-9878

DOI: 10.1039/C2DT30501A
Received 01 Mar 2012, Accepted 17 Jul 2012
First published online 17 Jul 2012

This article is part of themed collection: Polyoxometalates

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Abstract
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An unusual PFO₃²⁻-templated “inverse Keggin” polyanion, [Mo₁₂O₄₆(PF)₄]⁴⁻, has been isolated from the degradation reaction of an {Mo₁₃₂}-type Keplerate to [PMo₁₂O₄₀]³⁻ by [Cu(MeCN)₄](PF₆) in acetonitrile. ³¹P-NMR studies suggest a structure-directing role for [Cu(MeCN)₄]⁺ in the formation of the highly unusual all-inorganic inverse Keggin structure.

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