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Issue 9, 2012
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In situ time-resolved DXAFS study of Rh nanoparticle formation mechanism in ethylene glycol at elevated temperature

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Abstract

A combination of in situ time-resolved DXAFS and ICP-MS techniques reveals that the formation process of Rh nanoparticles (NPs) from rhodium trichloride trihydrate (RhCl3·3H2O) in ethylene glycol with polyvinylpyrrolidone (PVP) at elevated temperature is a first-order reaction, which indicates that uniform size Rh NPs appear consecutively and these Rh NPs do not aggregate with each other.

Graphical abstract: In situ time-resolved DXAFS study of Rh nanoparticle formation mechanism in ethylene glycol at elevated temperature

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Publication details

The article was received on 28 Sep 2011, accepted on 05 Dec 2011 and first published on 27 Jan 2012


Article type: Paper
DOI: 10.1039/C2CP23070D
Citation: Phys. Chem. Chem. Phys., 2012,14, 2983-2990
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    In situ time-resolved DXAFS study of Rh nanoparticle formation mechanism in ethylene glycol at elevated temperature

    H. Asakura, K. Teramura, T. Shishido, T. Tanaka, N. Yan, C. Xiao, S. Yao and Y. Kou, Phys. Chem. Chem. Phys., 2012, 14, 2983
    DOI: 10.1039/C2CP23070D

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