Issue 13, 2012
From the journal:

CrystEngComm

C–Br⋯O supramolecular synthon: in situ cryocrystallography of low melting halogen-bonded complexes†‡

Susanta K. Nayak,a   Giancarlo Terraneo,ab   Alessandra Forni,c   Pierangelo Metrangolo*ab  and  Giuseppe Resnati*ab  

* Corresponding authors

a Center for Nano Science and Technology@Polimi, Istituto Italiano di Tecnologia, Via Pascoli 70/3, 20133 Milan, Italy

b NFMLAB-DCMIC “Giulio Natta”, Politecnico di Milano, Via L. Mancinelli 7, 20131 Milan, Italy

c ISTM-CNR, Universita` di Milano, Via Venezian 21, I-20133 Milan, Italy
E-mail: pierangelo.metrangolo@polimi.it, giuseppe.resnati@polimi.it
Fax: +39 02 2399 3080
Tel: +39 02 2399 3041 (P. M.), 3032 (G. R.)

Abstract

In situ cryocrystallization of mixtures of 1,3-dibromotetrafluorobenzene and various oxygenated solvents afforded halogen bonded adducts. Single crystal X-ray analyses afforded structural information on the Br⋯O synthon and its role in driving the self-assembly process.

Graphical abstract: C–Br⋯O supramolecular synthon: in situ cryocrystallography of low melting halogen-bonded complexes

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Article information

DOI
https://doi.org/10.1039/C2CE25403D
Article type
Communication
Submitted
23 Jan 2012
Accepted
27 Mar 2012
First published
28 Mar 2012

CrystEngComm, 2012,14, 4259-4261

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C–Br⋯O supramolecular synthon: in situ cryocrystallography of low melting halogen-bonded complexes

S. K. Nayak, G. Terraneo, A. Forni, P. Metrangolo and G. Resnati, CrystEngComm, 2012, 14, 4259 DOI: 10.1039/C2CE25403D

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