Spontaneous resolution of a homochiral helix built from a tetra-nuclear nickel cluster

Wenxu Zheng; Yongqin Wei; Chong-bin Tian; Xueying Xiao; Kechen Wu

doi:10.1039/C2CE25108F

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CrystEngComm

Issue 10, 2012

Design and understanding of solid-state and crystalline materials

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Spontaneous resolution of a homochiral helix built from a tetra-nuclear nickel cluster

Wenxu Zheng,^a^b Yongqin Wei,^a Chong-bin Tian,^a Xueying Xiao^a and Kechen Wu*^a

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State Key Laboratory of Structure Chemistry, Fujian Institute of Research on the Structure of Matter, Chinese Academy of Sciences, Fuzhou, P. R. China
E-mail: wkc@fjirsm.ac.cn ;
Fax: +86-591-83792932 ;
Tel: +86-591-83792600

Graduate School of Chinese Academy of Sciences, Beijing 100039, P. R. China

CrystEngComm, 2012,14, 3347-3350

DOI: 10.1039/C2CE25108F
Received 24 Jan 2012, Accepted 02 Mar 2012
First published online 02 Mar 2012

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A chirally helical coordination polymer [Ni₄(H₂O)₇L₄·H₂O]_n (H₂L = 2-(pyridin-2-yl)-1H-imidazole-4,5-dicarboxylic acid) constructed from a Ni₄L₄ building block exhibits spontaneous chiral resolution and the enantiomers of 1M and 1P have been confirmed by single-crystal analysis and solid-state circular dichroism spectra. The magnetic properties of compound 1 are also discussed.

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Wenxu Zheng
Yongqin Wei
Chong-bin Tian
Xueying Xiao
Kechen Wu

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