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Issue 94, 2012
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Interconversion between different stoichiometric forms of a three-component crystal via liquid-assisted grinding

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Abstract

A second polymorphic form of a 1 : 2 : 3 pamoate : DABCO : water salt has been obtained by liquid-assisted grinding, and it is shown that interconversion between this salt and a salt with 1 : 1 : 2 stoichiometry is facile via liquid-assisted grinding with additional amounts of pamoic acid (to generate the 1 : 1 : 2 salt) or DABCO (to generate the 1 : 2 : 3 salt).

Graphical abstract: Interconversion between different stoichiometric forms of a three-component crystal via liquid-assisted grinding

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Publication details

The article was received on 30 Aug 2012, accepted on 27 Sep 2012 and first published on 09 Oct 2012


Article type: Communication
DOI: 10.1039/C2CC36313E
Citation: Chem. Commun., 2012,48, 11507-11509
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    Interconversion between different stoichiometric forms of a three-component crystal via liquid-assisted grinding

    L. Loots, H. Wahl, L. van der Westhuizen, D. A. Haynes and T. le Roex, Chem. Commun., 2012, 48, 11507
    DOI: 10.1039/C2CC36313E

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