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Issue 23, 2013
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Sequential [6+2], [2+2], and [3+2] annulations for rapid assembly of multiple fragments

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Abstract

Assembly of four components through sequential [6+2], [2+2], and [3+2] annulations on an azulenone manifold allows for five-step access to a natural product-inspired scaffold with exquisite control of the ten consecutive stereocenters. X-ray analysis was used to define the spatial arrangement of the three fragments and functional groups on this rigid scaffold.

Graphical abstract: Sequential [6+2], [2+2], and [3+2] annulations for rapid assembly of multiple fragments

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Publication details

The article was received on 11 Dec 2012, accepted on 07 Jan 2013 and first published on 07 Jan 2013


Article type: Communication
DOI: 10.1039/C2CC38854E
Citation: Chem. Commun., 2013,49, 2299-2301
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    Sequential [6+2], [2+2], and [3+2] annulations for rapid assembly of multiple fragments

    V. Mahendar, H. Oikawa and H. Oguri, Chem. Commun., 2013, 49, 2299
    DOI: 10.1039/C2CC38854E

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