[18F]Fluorination of an arylboronic ester using [18F]selectfluor bis(triflate): application to 6-[18F]fluoro-L-DOPA

Ida S. R. Stenhagen; Anna K. Kirjavainen; Sarita J. Forsback; Charlotte G. Jørgensen; Edward G. Robins; Sajinder K. Luthra; Olof Solin; Véronique Gouverneur

doi:10.1039/C2CC38646A

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Chemical Communications

Issue 14, 2013

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[¹⁸F]Fluorination of an arylboronic ester using [¹⁸F]selectfluor bis(triflate): application to 6-[¹⁸F]fluoro-L-DOPA

Ida S. R. Stenhagen,^a Anna K. Kirjavainen,^b Sarita J. Forsback,^b Charlotte G. Jørgensen,^a Edward G. Robins,^c Sajinder K. Luthra,^c Olof Solin^b and Véronique Gouverneur*^a

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Chemistry Research Laboratory, University of Oxford, 12 Mansfield Road, Oxford, UK
E-mail: veronique.gouverneur@chem.ox.ac.uk ;
Fax: +44 (0)1865 285002 ;
Tel: +44 (0)1865 276544

Turku PET Centre, Radiopharmaceutical Chemistry Laboratory, Kiinamyllynkatu 4-8, FIN-20520 Turku, Finland

The Grove Centre, White Lion Road, Amersham, UK

Chem. Commun., 2013,49, 1386-1388

DOI: 10.1039/C2CC38646A
Received 02 Dec 2012, Accepted 02 Jan 2013
First published online 03 Jan 2013

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The Ag-mediated electrophilic [¹⁸F]fluorination of an arylboronic ester is reported. This new radiochemical transformation uses [¹⁸F]selectfluor bis(triflate) in acetone. The process gave 6-[¹⁸F]fluoro-L-DOPA with a RCY of 19 ± 12% and a specific activity of 2.6 ± 0.3 GBq μmol⁻¹.

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Ida S. R. Stenhagen
Anna K. Kirjavainen
Sarita J. Forsback
Charlotte G. Jørgensen
Edward G. Robins
Sajinder K. Luthra
Olof Solin
Véronique Gouverneur

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Chemical Communications

[¹⁸F]Fluorination of an arylboronic ester using [¹⁸F]selectfluor bis(triflate): application to 6-[¹⁸F]fluoro-L-DOPA

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Chemical Communications

[18F]Fluorination of an arylboronic ester using [18F]selectfluor bis(triflate): application to 6-[18F]fluoro-L-DOPA

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[¹⁸F]Fluorination of an arylboronic ester using [¹⁸F]selectfluor bis(triflate): application to 6-[¹⁸F]fluoro-L-DOPA