A stable and strongly luminescent dinuclear Cu(I) helical complex prepared from 2-diphenylphosphino-6-methylpyridine

Juan-José Cid; John Mohanraj; Meera Mohankumar; Michel Holler; Gianluca Accorsi; Lydia Brelot; Iwona Nierengarten; Omar Moudam; Adrien Kaeser; Béatrice Delavaux-Nicot; Nicola Armaroli; Jean-François Nierengarten

doi:10.1039/C2CC37873F

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Chemical Communications

Issue 9, 2013

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A stable and strongly luminescent dinuclear Cu(I) helical complex prepared from 2-diphenylphosphino-6-methylpyridine

Juan-José Cid,^a John Mohanraj,^b Meera Mohankumar,^a Michel Holler,^a Gianluca Accorsi,^b Lydia Brelot,^c Iwona Nierengarten,^a^c Omar Moudam,^a^d Adrien Kaeser,^a^d Béatrice Delavaux-Nicot,*^d Nicola Armaroli*^b and Jean-François Nierengarten*^a

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Laboratoire de Chimie des Matériaux Moléculaires, Université de Strasbourg et CNRS (UMR 7509), 25 rue Becquerel, 67087 Strasbourg Cedex 2, France
E-mail: nierengarten@unistra.fr

Istituto per la Sintesi Organica e la Fotoreattività/CNR, Via Gobetti 101, 40129 Bologna, Italy
E-mail: nicola.armaroli@isof.cnr.it

Service de RX, Institut de Chimie, Université de Strasbourg, BP 296/R8, 67008 Strasbourg Cedex, France

Laboratoire de Chimie de Coordination du CNRS (UPR 8241), Université de Toulouse (UPS, INP), 205 Route de Narbonne, 31077 Toulouse, France
E-mail: beatrice.delavaux-nicot@lcc-toulouse.fr

Chem. Commun., 2013,49, 859-861

DOI: 10.1039/C2CC37873F
Received 30 Oct 2012, Accepted 30 Nov 2012
First published online 30 Nov 2012

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Treatment of 2-diphenylphosphino-6-methylpyridine (dpPyMe) with Cu(CH₃CN)₄BF₄ afforded the stable dinuclear Cu(I) complex [Cu₂(μ-dpPyMe)₃(CH₃CN)](BF₄)₂. This compound is a weak emitter in solution, however a remarkably high emission quantum yield (46%) has been found in a rigid matrix at room temperature.

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Chemical Communications

A stable and strongly luminescent dinuclear Cu(I) helical complex prepared from 2-diphenylphosphino-6-methylpyridine

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A stable and strongly luminescent dinuclear Cu(I) helical complex prepared from 2-diphenylphosphino-6-methylpyridine

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