Pd-catalysed direct dehydrogenative carboxylation of alkenes: facile synthesis of vinyl esters

Dan Yang; Shixuan Ding; Jianhui Huang; Kang Zhao

doi:10.1039/C2CC37779A

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Chemical Communications

Issue 12, 2013

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Pd-catalysed direct dehydrogenative carboxylation of alkenes: facile synthesis of vinyl esters

Dan Yang,^a Shixuan Ding,^a Jianhui Huang*^a and Kang Zhao*^a

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Tianjin Key Laboratory for Modern Drug Delivery & High-Efficiency, School of Pharmaceutical Science and Technology, Tianjin University, Tianjin 300072, China
E-mail: jhuang@tju.edu.cn, kangzhao@tju.edu.cn ;
Fax: +86-22-27404031 ;
Tel: +86-22-27405316

Chem. Commun., 2013,49, 1211-1213

DOI: 10.1039/C2CC37779A
Received 26 Oct 2012, Accepted 20 Dec 2012
First published online 20 Dec 2012

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A novel Pd-catalysed oxidative coupling reaction methodology using readily available carboxylic acids and alkenes for the preparation of vinyl esters has been developed. A broad range of vinyl esters were successfully synthesised. The reactions have demonstrated good efficiency as well as excellent chemo- and regio-selectivity.

Abstract from Catalysts & Catalysed Reactions 2013

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