Formation of a pillar[5]arene-based [3]pseudorotaxane in solution and in the solid state

Lingyan Gao; Chengyou Han; Bo Zheng; Shengyi Dong; Feihe Huang

doi:10.1039/C2CC37646F

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Chemical Communications

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Formation of a pillar[5]arene-based [3]pseudorotaxane in solution and in the solid state

Lingyan Gao,^a Chengyou Han,^a Bo Zheng,^a Shengyi Dong^a and Feihe Huang*^a

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MOE Key Laboratory of Macromolecular Synthesis and Functionalization, Department of Chemistry, Zhejiang University, Hangzhou 310027, P. R. China
E-mail: fhuang@zju.edu.cn ;
Fax: +86-571-8795-3189 ;
Tel: +86-571-8795-3189

Chem. Commun., 2013,49, 472-474

DOI: 10.1039/C2CC37646F
Received 20 Oct 2012, Accepted 20 Nov 2012
First published online 20 Nov 2012

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Abstract
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It was demonstrated that a novel [3]pseudorotaxane could be separated by column chromatography during the synthesis of a copillar[5]arene. Single crystal X-ray analysis revealed that this [3]pseudorotaxane consisted of the copillar[5]arene and its monomer in a molar ratio of 2:1.