Antiferromagnetic ordering through a hydrogen-bonded network in the molecular solid CuF2(H2O)2(3-chloropyridine)

Saul H. Lapidus; Jamie L. Manson; Hyunsoo Park; Alexander J. Clement; Saman Ghannadzadeh; Paul Goddard; Tom Lancaster; Johannes S. Möller; Stephen J. Blundell; Mark T. F. Telling; Jinhee Kang; Myung-Hwan Whangbo; John A. Schlueter

doi:10.1039/C2CC37444G

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Chemical Communications

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Antiferromagnetic ordering through a hydrogen-bonded network in the molecular solid CuF₂(H₂O)₂(3-chloropyridine)

Saul H. Lapidus,^a Jamie L. Manson,^b Hyunsoo Park,^a Alexander J. Clement,^a Saman Ghannadzadeh,^c Paul Goddard,^c Tom Lancaster,^d Johannes S. Möller,^c Stephen J. Blundell,^c Mark T. F. Telling,^e^f Jinhee Kang,^g Myung-Hwan Whangbo^g and John A. Schlueter*^a

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Materials Science Division, Argonne National Laboratory, Argonne, USA
E-mail: JASchlueter@anl.gov ;
Fax: +1-630-252-9555 ;
Tel: +1-630-252-3588

Department of Chemistry and Biochemistry, Eastern Washington University, Cheney, USA

University of Oxford, Department of Physics, Clarendon Laboratory, Parks Road, Oxford OX1 3PU, UK

Centre for Materials Physics, Durham University, South Road, Durham, UK

ISIS Facility, Rutherford Appleton Laboratory, Chilton, UK

Department of Materials, University of Oxford, Parks Road, Oxford, UK

Department of Chemistry, North Carolina State University, Raleigh, USA

Chem. Commun., 2013,49, 499-501

DOI: 10.1039/C2CC37444G
Received 12 Oct 2012, Accepted 18 Nov 2012
First published online 20 Nov 2012

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CuF₂(H₂O)₂(3-chloropyridine) possesses a five-coordinate Cu²⁺ center with a slightly distorted trigonal bypyramidal coordination geometry. Strong intermolecular FH–O hydrogen bonds enable the formation of 2D layers and provide the primary magnetic exchange path that leads to the stabilization of long-range antiferromagnetic (AFM) order below T_N = 2.1 K.

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Chemical Communications

Antiferromagnetic ordering through a hydrogen-bonded network in the molecular solid CuF₂(H₂O)₂(3-chloropyridine)

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Antiferromagnetic ordering through a hydrogen-bonded network in the molecular solid CuF2(H2O)2(3-chloropyridine)

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Antiferromagnetic ordering through a hydrogen-bonded network in the molecular solid CuF₂(H₂O)₂(3-chloropyridine)