Iridium(III) azuliporphyrins

Timothy D. Lash; Komal Pokharel; Matthias Zeller; Gregory M. Ferrence

doi:10.1039/C2CC37104A

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Chemical Communications

Issue 96, 2012

Urgent high quality communications from across the chemical sciences.

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Iridium(III) azuliporphyrins

Timothy D. Lash,*^a Komal Pokharel,^a Matthias Zeller^b and Gregory M. Ferrence^a

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Department of Chemistry, Illinois State University, Normal, Illinois 61790-4160, USA
E-mail: tdlash@ilstu ;
Fax: +1 (309) 438-5538 ;
Tel: +1 (309) 438-8554

Department of Chemistry, Youngstown State University, One University Plaza, Youngstown, USA

Chem. Commun., 2012,48, 11793-11795

DOI: 10.1039/C2CC37104A
Received 29 Sep 2012, Accepted 19 Oct 2012
First published online 22 Oct 2012

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Azuliporphyrins were reacted with [Ir(COD)Cl]₂ in refluxing o- or p-xylene to give novel iridium(III) derivatives that regioselectively incorporated an oxidized solvent molecule. The iridium(III) is inserted within the porphyrinoid macrocycle and possesses an additional apical acyl unit.

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