Molybdate templated assembly of Ln12Mo4-type clusters (Ln = Sm, Eu, Gd) containing a truncated tetrahedron core

Yong Zheng; Qian-Chong Zhang; La-Sheng Long; Rong-Bin Huang; Achim Müller; Jürgen Schnack; Lan-Sun Zheng; Zhiping Zheng

doi:10.1039/C2CC36530H

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Chemical Communications

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Molybdate templated assembly of Ln₁₂Mo₄-type clusters (Ln = Sm, Eu, Gd) containing a truncated tetrahedron core

Yong Zheng,^a Qian-Chong Zhang,^a La-Sheng Long,*^a Rong-Bin Huang,^a Achim Müller,^b Jürgen Schnack,^c Lan-Sun Zheng^a and Zhiping Zheng^a

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State Key Laboratory of Physical Chemistry of Solid Surface and Department of Chemistry, College of Chemistry and Chemical Engineering, Xiamen University, Xiamen 361005, China
E-mail: lslong@xmu.edu.cn ;
Fax: +86 592 218 3047

Faculty of Chemistry, University of Bielefeld, P.O. Box 10 0131, D-33501 Bielefeld, Germany

Faculty of Physics, University of Bielefeld, P.O. Box 10 0131, D-33501 Bielefeld, Germany

Chem. Commun., 2013,49, 36-38

DOI: 10.1039/C2CC36530H
Received 07 Sep 2012, Accepted 16 Oct 2012
First published online 16 Oct 2012

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Three heterometallic cluster complexes {Ln₁₂Mo₄} featuring an Ln₁₂ core of a distorted truncated tetrahedron were synthesized with the assistance of four MoO₄²⁻ anions as ancillary ligands. Magnetic studies of the {Gd₁₂Mo₄} cluster revealed a large magnetocaloric effect due to the presence of the large number of weakly coupled Gd(III) ions.

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Yong Zheng
Qian-Chong Zhang
La-Sheng Long
Rong-Bin Huang
Achim Müller
Jürgen Schnack
Lan-Sun Zheng
Zhiping Zheng

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Chemical Communications

Molybdate templated assembly of Ln₁₂Mo₄-type clusters (Ln = Sm, Eu, Gd) containing a truncated tetrahedron core

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Molybdate templated assembly of Ln12Mo4-type clusters (Ln = Sm, Eu, Gd) containing a truncated tetrahedron core

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Molybdate templated assembly of Ln₁₂Mo₄-type clusters (Ln = Sm, Eu, Gd) containing a truncated tetrahedron core