High rate delithiation behaviour of LiFePO4 studied by quick X-ray absorption spectroscopy

Xiqian Yu; Qi Wang; Yongning Zhou; Hong Li; Xiao-Qing Yang; Kyung-Wan Nam; Steven N. Ehrlich; Syed Khalid; Ying Shirley Meng

doi:10.1039/C2CC36382H

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Chemical Communications

Issue 94, 2012

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High rate delithiation behaviour of LiFePO₄ studied by quick X-ray absorption spectroscopy

Xiqian Yu,^a Qi Wang,^a Yongning Zhou,^a Hong Li,^b Xiao-Qing Yang,*^a Kyung-Wan Nam,*^a Steven N. Ehrlich,^a Syed Khalid^a and Ying Shirley Meng^c

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Corresponding authors

Brookhaven National Laboratory, Upton, USA
E-mail: xyang@bnl.gov ;
Tel: +1-631-3443663

Institute of Physics, Chinese Academy of Sciences, Beijing, China

Department of NanoEngineering, University of California San Diego, La Jolla, USA

Chem. Commun., 2012,48, 11537-11539

DOI: 10.1039/C2CC36382H
Received 01 Sep 2012, Accepted 08 Oct 2012
First published online 09 Oct 2012

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A novel in situ time-resolved synchrotron X-ray absorption spectroscopy (XAS) was introduced for the dynamic studies during fast chemical and electrochemical delithiation of LiFePO₄. The lithium diffusion in LiFePO₄ and the reaction mechanisms for both processes were investigated. This approach opens new opportunities for dynamic studies of various energy storage systems.

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Xiqian Yu
Qi Wang
Yongning Zhou
Hong Li
Xiao-Qing Yang
Kyung-Wan Nam
Steven N. Ehrlich
Syed Khalid
Ying Shirley Meng

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