Interconversion between different stoichiometric forms of a three-component crystal via liquid-assisted grinding

Leigh Loots; Helene Wahl; Leandi van der Westhuizen; Delia A. Haynes; Tanya le Roex

doi:10.1039/C2CC36313E

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Chemical Communications

Issue 94, 2012

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Communication

Interconversion between different stoichiometric forms of a three-component crystal via liquid-assisted grinding

Leigh Loots,^a Helene Wahl,^a Leandi van der Westhuizen,^a Delia A. Haynes*^a and Tanya le Roex*^a

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Department of Chemistry and Polymer Science, University of Stellenbosch, P. Bag X1, Matieland, Republic of South Africa
E-mail: dhaynes@sun.ac.za

Chem. Commun., 2012,48, 11507-11509

DOI: 10.1039/C2CC36313E
Received 30 Aug 2012, Accepted 27 Sep 2012
First published online 09 Oct 2012

This article is part of themed collection: Mechanochemistry: fundamentals and applications in synthesis

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A second polymorphic form of a 1:2:3 pamoate:DABCO:water salt has been obtained by liquid-assisted grinding, and it is shown that interconversion between this salt and a salt with 1:1:2 stoichiometry is facile via liquid-assisted grinding with additional amounts of pamoic acid (to generate the 1:1:2 salt) or DABCO (to generate the 1:2:3 salt).