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Department of Synthetic and Biological Chemistry, Graduate School of Engineering, Kyoto University, Nishikyo-ku, 615-8510 Kyoto, Japan
; Fax: +81-75-383-2725
; Tel: +81-75-383-2726
Chem. Commun., 2012,48, 11211-11213
26 Aug 2012,
27 Sep 2012
First published online
28 Sep 2012
We found that an integrated flow microreactor system enables the preparation of boronic esters bearing electrophilic functional groups using organolithium chemistry and that it allows for their use in Suzuki–Miyaura cross-coupling without intentionally added base. Based on this method, cross-coupling of two aryl halides bearing electrophilic functional groups was accomplished to obtain the corresponding biaryl compounds in one flow.
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